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Analytical Sciences: X-ray Structure Analysis Online
Vol. 24 (2008) P x89-x90

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http://doi.org/10.2116/analscix.24.x89

Part 5

The title compound, [Ag(Phca2en)(PPh3)2]ClO4, where Phca2en is N,N′-bis(β-phenylcinnamaldehyde)ethylenediimine, crystallizes in space group P21/n, with a = 21.2044(7), b = 10.5089(3), c = 28.1172(9)Å, β = 109.205(1)°, V = 5916.8(3)Å3, Z = 4, T = 292 K, Dcalc = 1.386 mg m-3. The coordination polyhedron about the Ag(I) atom is a distorted AgN2P2 tetrahedron and the Phca2en acts as an N,N′-bidentate ligand.

Copyright © 2008 by The Japan Society for Analytical Chemistry

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