Bulletin of the Chemical Society of Japan
Online ISSN : 1348-0634
Print ISSN : 0009-2673
ISSN-L : 0009-2673
Extractive Separation and Photometric Determination of Vanadium with Benzoylacetone
Rakam Singh ChauhanLajpat Rai Kakkar
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1992 Volume 65 Issue 4 Pages 1033-1037

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Abstract

A very simple and rapid method for the extractive separation and photometric determination of vanadium is worked out using benzoylacetone as a complexing reagent for V(III), produced on reduction of V(V) with sodium dithionite in dil acetic acid medium. The colored complex is extractable into benzene. The interfering effect of a large number of elements is eliminated completely leading directly to the determination of the metal ion present in traces in samples. The method is applicable to the analysis of different technical samples and the results obtained are highly reproducible. Metal to ligand ratio in the extracted species is determined as 1 : 3.

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© 1992 The Chemical Society of Japan
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