Bulletin of the Chemical Society of Japan
Online ISSN : 1348-0634
Print ISSN : 0009-2673
ISSN-L : 0009-2673
 
Intramolecular Photocycloaddition of 2-(2-Alkenyloxymethyl)naphthalene-1-carbonitriles Using Glass-Made Microreactors
Hirofumi MukaeHajime MaedaSatoshi NashiharaKazuhiko Mizuno
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2007 Volume 80 Issue 6 Pages 1157-1161

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Abstract

Intramolecular [2+2] and [2+3] photocycloadditions of 2-(2-alkenyloxymethyl)naphthalene-1-carbonitriles and their photocycloreversion using glass-made microreactors were investigated in comparison with photoreactions under conventional batch conditions. Both the efficiency and regioselectivity were improved by use of glass-made microreactors. These results can be explained by thorough absorption of light and outflow of primary product from the reaction system.

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© 2007 The Chemical Society of Japan
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