Bulletin of the Chemical Society of Japan
Online ISSN : 1348-0634
Print ISSN : 0009-2673
ISSN-L : 0009-2673
Alkali Fusion-Gas Chromatography of Alkyl Sulfates
Terumichi NakagawaKoichiro MiyajimaToyozo Uno
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1968 Volume 41 Issue 12 Pages 2899-2903

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Abstract

The alkali fusion of alkyl sulfates was investigated by pyrolyzing a mixture of alkyl sulfates and alkali metal hydroxide between 200–500°C. The pyrolyzates were isolated and identified to be 1-olefins, internal olefins, alcohols, and dialkyl ethers by gas chromatography and IR spectroscopy. The mechanism of this reaction was proposed from these results and an attempt was carried out to estimate the alkyl chain carbon number distribution of the commercially available sodium alkyl sulfates.

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