Bulletin of the Chemical Society of Japan
Online ISSN : 1348-0634
Print ISSN : 0009-2673
ISSN-L : 0009-2673
Synthesis of (±)-Tetrahydroanhydroaucubigenone and (±)-Tetrahydroanhydroaucubigenin
Heitaro ObaraHiroshi KimuraMasanobu SuzukiJun-ichi Onodera
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1978 Volume 51 Issue 12 Pages 3610-3611

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Abstract

The racemate of tetrahydroanhydroaucubigenone (3), one of the related compounds of aucubin, was synthesized by the photoirradiation of 6-[2-(nitrosooxy)ethyl]-3-oxabicyclo[3.3.0]octan-7-one. (±)-Tctrahydroanhydroaucubigenin was also obtained by reduction of (±)-3 with sodium in moist ether.

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