Bulletin of the Chemical Society of Japan
Online ISSN : 1348-0634
Print ISSN : 0009-2673
ISSN-L : 0009-2673
The Thermal Decomposition of N,O-Diacyl-N-t-butylhydroxylamines
Yuzuru UchidaYukinobu HashimotoSeizi Kozuka
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1980 Volume 53 Issue 8 Pages 2309-2314

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Abstract

Several N,O-diacyl-N-t-butylhydroxylamines and O-acyl-N-t-butylhydroxylamines were prepared, and their thermal decompositions were studied. The thermal decompositions of N,O-diacyl-N-t-butylhydroxylamines in tetralin gave substituted N-t-butylbenzamides, carboxylic acids, 1,1′-bitetralyl, and 1,2-dihydronaphthalene as the major products, together with small amounts of carbon dioxide, t-butylamine, and benzanilides. In the thermal decompositions of O-acyl-N-t-butylhydroxylamines, the products were t-butylamine, carboxylic acids, substituted N-t-butylbenzamides, 1,1′-bitetralyl, and 1,2-dihydronaphthalene.

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