1980 Volume 53 Issue 8 Pages 2322-2326
Reaction of the title compound with acetylacetone in the presence of a catalytic amount of sodium hydroxide afforded the 2-C-diacetylmethyl and 2-C-acetylmethyl derivatives having the altro, gluco, and manno configurations. The 2-C-diacetylmethyl derivative with the altro configuration exceptionally exists in a skew boat form. The product ratio depends on solvent and the amount of THF.
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