Bulletin of the Chemical Society of Japan
Online ISSN : 1348-0634
Print ISSN : 0009-2673
ISSN-L : 0009-2673
A Convenient Reduction Method of β-Phenyl α,β-Unsaturated Carbonyl Compounds with Me3SiCl–NaI–ROH Reagent
Takashi SakaiKazuyoshi MiyataMasanori UtakaAkira Takeda
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1987 Volume 60 Issue 3 Pages 1063-1066

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Abstract

Treatment of β-phenyl α,β-unsaturated ketones, cinnamic acid and its ester with Me3SiCl–NaI–ROH reagent in hexane at room temperature gave the corresponding saturated carbonyl compounds in good yields. A similar reaction of 2,4-hexadienoic acid afforded 4-hexanolide.

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