Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
A Tetranuclear Vanadium(III, III, IV, IV) Complex Formed by a Reaction of Bis(acetylacetonato)oxovanadium(IV) with a Thiolate Ligand
Masahiro MikuriyaTakanori KoteraFumiya AdachiShunji Bandow
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1993 Volume 22 Issue 6 Pages 945-948

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Abstract

A mixed-valence tetranuclear vanadium(III, III, IV, IV) complex, [V2(VO)2(acac)4(CH3O)6] (Hacac = acetylacetone), has been isolated by a reaction of VO(acac)2 with 2-(3-aminopropylamino)ethanethiol in methanol-dichloromethane. The complex has been characterized by X-ray structure analysis, XPS and electronic spectra, and magnetic susceptibilities (80–300 K).

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© 1993 The Chemical Society of Japan
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