Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Synthesis and Characterization of Tetraethylethanediselenoamide
Juzo NakayamaAyako MizumuraIsao AkiyamaTakehiko NishioIkuo Iida
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1994 Volume 23 Issue 1 Pages 77-80

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Abstract

Tetraethylethanediselenoamide (2) was prepared in 81% yield by reaction of tetraethylethynediamine with elemental selenium. The X-ray single crystal structure analysis revealed that two Et2N(C=Se)– units of 2 are perpendicular to each other. The oxidation of 2 with m-CPBA produced tetraethylmonoselenooxamide and the reaction with DMAD afforded dimethyl 4,5-bis(diethylamino)selenophene-2,3-dicarboxylate.

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© 1994 The Chemical Society of Japan
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