Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Potassium Exchanged Layered Zirconium Phosphate as Base Catalyst in the Synthesis of 2-Nitroalkanols
U. CostantinoM. CuriniF. MarmottiniO. RosatiE. Pisani
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1994 Volume 23 Issue 12 Pages 2215-2218

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Abstract

The synthesis of 2-nitroalkanols from nitroalkanes and aldehydes occurs efficiently, in mild conditions without solvent, when mediated by layered Zr(KOPO3)2. The reaction has been tested in the preparation of ten different nitroalkanols and the data obtained seem to indicate that not only the surface but also the interlayer ≡P–OK+ groups are involved in the catalytic process.

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© 1994 The Chemical Society of Japan
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