Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Direct and Electrophilic Preparation of α-Thiocyanatoketones and Aldehydes Using Thiocyanatotrimethylsilane and Sulfuryl Chloride
Yoo TanabeTakuya MakitaKei Mori
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1994 Volume 23 Issue 12 Pages 2275-2278

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Abstract

The thiocyanato (-SCN) group was directly and regioselectively introduced into the α-position of ketones, aldehydes, and aldols in an electrophilic manner by the combined use of thiocyanatotrimethylsilane and sulfuryl chloride with or without cyclic sec-amine catalysts under mild reaction conditions.

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© 1994 The Chemical Society of Japan
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