Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Selective Electrochemical Formyl Hydrogen-Exchange Fluorination of Aliphatic Aldehydes to Prepare Acyl Fluorides Using HF-Base Solutions
Norihiko YonedaSheng-Qi ChenTsuyoshi HatakeyamaSyoji HaraTsuyoshi Fukuhara
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1994 Volume 23 Issue 5 Pages 849-850

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Abstract

The selective displacement of formyl hydrogen (–(C=O)–H) to fluorine in aliphatic aldehydes was successfully carried out electrochemically to give acyl fluorides in base-nHF (base: pyridine or Et3N, n = 3–6) electrolyte solution with or without solvents such as acetonitrile and sulfolane.

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© 1994 The Chemical Society of Japan
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