Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
A Regioselective Synthesis of 6-Deoxyanthracyclinone Intermediate
Hiroshi TanakaTakeo Yoshioka
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1994 Volume 23 Issue 5 Pages 953-956

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Abstract

A new route for synthesis of 6-deoxyanthracyclinone has been developed. Preparation of the key intermediate 2-ethylenedioxy-9-pivaloyloxy-1,2,3,4-tetrahydroanthracene-5,8-dione was achieved by chemoselective reduction of the adduct of naphthazarin monopivalate with 1-methoxy-3-trimethylsiloxybutadiene, and successive dehydration of the resulting alcohol.

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© 1994 The Chemical Society of Japan
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