Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
The Formation of Monomethyl Carbonato-bridged Dinuclear Nickel(II) Complexes by an Efficient CO2 Uptake in Methanol Containing Urea Derivatives
Yoko HosokawaHeitaro YamaneYasuo NakaoKeiji MatsumotoSatoshi TakamizawaWasuke MoriShinnichiro Suzuki
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1997 Volume 26 Issue 9 Pages 891-892

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Abstract

Monomethyl carbonato-bridged dinuclear nickel(II) complexes [Ni2(L)(OOC-O-CH3)(CH3OH)2](ClO4)2·H2O·CH3OH, 1 and [Ni2(L)(OOC-O-CH3)(H2O)2](ClO4)2·H2O, 2 were obtained in the presence of [Ni2(L)(OH)(H2O)2](ClO4)2 and N-methylurea at room temperature in air, where HL is N,N,N′,N′-tetrakis[(1-ethyl-2-benzimidazolyl)methyl]- 2-hydroxy-1,3-diaminopropane. The crystal structure of 1 was determined by X-ray crystallography and 2 was characterized by the magnetic susceptibility and visible absorption spectrum.

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© 1997 The Chemical Society of Japan
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