Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
Nucleophilic Allylation-Heterocyclization via Bis-π-allylpalladium Complexes: Synthesis of Five- and Six-Membered Heterocycles
Ming BaoHiroyuki NakamuraAkihiko InoueYoshinori Yamamoto
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Volume 31 (2002) Issue 2 Pages 158-159

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Abstract

The reaction of the allylic halides 59 having an aldehyde or an imine moiety in the molecule with allyltributylstannane proceeded smoothly in the presence of Pd2•dba3•CHCl3 (5 mol%) in DMF or THF, giving the corresponding heterocycles 1014 in good to high yields. The Stille coupling product was not obtained under these reaction conditions.

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© 2002 The Chemical Society of Japan
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