Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Letter
Reductive Etherification under Microfluidic Conditions: Application to Practical Synthesis of the FGHIJ-Ring System of Yessotoxin
Tohru OishiTomoyoshi ImaizumiMichio Murata
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2010 Volume 39 Issue 2 Pages 108-109

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Abstract

Reductive etherification, a key reaction for constructing the H-ring in the convergent synthesis of the FGHIJ-ring system of yessotoxin, was problematic because the yield dramatically decreased upon increasing the scale of the reaction. This issue was solved by the use of a microflow reactor, and a gram scale reaction was successfully performed.

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© 2010 The Chemical Society of Japan
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