2012 Volume 41 Issue 12 Pages 1678-1680
A 24-membered cyclic decanedisulfide dimer (1,2,13,14-tetrathiacyclotetracosane) was effectively synthesized by resin-supported cyclization of 1,10-decanedithiol. Despite the formation of a series of cyclic oligomers, no monomeric decanedisulfide resulted. The crystal structure of the dimeric macrocycle was reported.
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