Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Letter
Enantioselective Recognition of [60]Fullerene Bisadducts by Cyclodextrin: Kinetic Control of a Mechanochemical High-speed Vibration Milling Process
Atsushi IkedaMichiko IshikawaJun-ichi KikuchiKazuyuki Nobusawa
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2013 Volume 42 Issue 10 Pages 1137-1139

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Abstract

The enantiomers of some fullerene bisadducts were separated by complexation with γ-cyclodextrin (γ-CDx) in a mechanochemical high-speed vibration milling (HSVM) apparatus, followed by decomplexation with the addition of DMSO. HSVM treatment, which is generally used for pharmaceutical preparation, was found to be governed not by thermodynamic control but by kinetic control.

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© 2013 The Chemical Society of Japan
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