Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
Acid-Catalyzed Autoxidation of 12-Hydroxyeudesman-3,6-dione to 6,12-Epoxyeudesma-4,6-dien-3-one
Hajime NaganoHiroko SugiharaHiroko ItoMichio Shiota
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1987 Volume 16 Issue 8 Pages 1571-1574

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Abstract

Treatment of a benzene solution of 12-hydroxyeudesman-3,6-dione with p-toluenesulfonic acid in air gave 6,12-epoxyeudesma-4,6-dien-3-one (2) in 57% yield. Dienone 2 was further oxidized to give 7-hydroxyeudesmanes.

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