Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
A Convenient Synthesis of Fluorine-Containing Highly-Substituted Furans through New Fluoride Ion-Catalyzed Reaction of 1-Alkyl-F-1-alkenyl Phosphates
Manabu KuroboshiTakao ShinozakiTakashi IshiharaTeiichi Ando
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1987 Volume 16 Issue 8 Pages 1621-1622

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Abstract

1-Alkyl-F-1-alkenyl phosphates, easily prepared from alkyl F-alkyl ketones and sodium diethyl phosphite, underwent the dephosphorylation followed by cyclocondensation in the presence of a fluoride ion catalyst and triethylamine at ambient temperature to give 3,4-di-F-alkylated furan derivatives in moderate to good yields.

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