Chemistry Letters
Online ISSN : 1348-0715
Print ISSN : 0366-7022
ISSN-L : 0366-7022
A NOVEL ELECTROSYNTHESIS OF α,α-DIMETHOXYALKANOATES FROM α-(2-BENZOTHIAZOLYLTHIO)ALKANOATES
Sigeru ToriiHirosi OkumotoHideo Tanaka
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1980 Volume 9 Issue 6 Pages 617-618

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Abstract

An efficient preparation of α,α-dimethoxyalkanoates (2) has been performed by electrolytic desulfurization of α-(2-benzothiazolylthio) alkanoates (1) in MeOH containing CuCl2 as a catalytic additive, yielding 2 (94–57%) together with disulfide 3 (88–48%).

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© The Chemical Society of Japan
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