Synthesis of (Z)-N-[5-(3-Aryl)-[1, 2, 4]oxadiazolyl]-N-[(methylcarbamoyl)methyl]benzamidoximes

Kazuho HARADA; Jun-ichi YOKOYAMA; Hiroaki TAKAYANAGI; Haruo OGURA; Shonosuke ZEN

doi:10.1248/cpb.40.1610

Chemical and Pharmaceutical Bulletin

Online ISSN : 1347-5223
Print ISSN : 0009-2363

Synthesis of (Z)-N-[5-(3-Aryl)-[1, 2, 4]oxadiazolyl]-N-[(methylcarbamoyl)methyl]benzamidoximes

Kazuho HARADA, Jun-ichi YOKOYAMA, Hiroaki TAKAYANAGI, Haruo OGURA, Shonosuke ZEN

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Keywords: primary nitro alkane, nitrile oxide, glycociamidine, [1, 2, 4]oxadiazole, 1, 3-dipolar cycloaddition, X-ray analysis

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Volume 40 (1992) Issue 6 Pages 1610-1611

DOI https://doi.org/10.1248/cpb.40.1610

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Abstract

(Z)-N-[5-(3-Aryl)-[1, 2, 4]oxadiazoly]-N-[(methylcarbamoyl)methyl]benzamidoximes (3) were synthesized through the reaction of 3-methylglycociamidine (2) with primary nitroalkanes (1) and acetyl chloride. The structural determination of 3 by single crystal X-ray analysis is reported.

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