Chemical and Pharmaceutical Bulletin
Online ISSN : 1347-5223
Print ISSN : 0009-2363
ISSN-L : 0009-2363
Bile Acids and Steroids. XIV. Thiosteroids. (3). Reduction of the 11β, 12β-Episulfide
Ken'ichi Takeda, Taichiro Komeno, Jun'ichi Kawanami
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1960 Volume 8 Issue 7 Pages 621-625

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Abstract
Treatment of methyl 3α-acetoxy-11β-thiocyanato-12α-chloro(or-mesyloxy)cholanate with alkali or lithium aluminium hydride afforded 11β, 12β-episulfides, which could not be further reduced to the 11β-thiol by various reagents.
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© The Pharmaceutical Society of Japan
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