Electrochemistry
Online ISSN : 2186-2451
Print ISSN : 1344-3542
ISSN-L : 1344-3542
Note
Highly Regioselective Anodic Monofluorination of 3H-1,4-Benzoxathian-2-ones in Et4NF·4HF/MeCN
Takuya SAKANASHIShinsuke INAGIToshio FUCHIGAMI
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JOURNALS OPEN ACCESS

2008 Volume 76 Issue 12 Pages 896-899

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Abstract

Highly regioselective anodic monofluorination of 3H-1,4-benzoxathian-2-ones was successfully carried out using anodically stable Et4NF·4HF as supporting electrolyte and fluorine source to provide the corresponding monofluorinated products in good yields while anodically less stable supporting electrolyte, Et3N·3HF, gave only poor yields.

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© 2008 The Electrochemical Society of Japan
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