Electrochemistry
Online ISSN : 2186-2451
Print ISSN : 1344-3542
ISSN-L : 1344-3542
Review (Invited Paper)
Measurement Methods on Electrodes and Electrocatalysts for Water Electrolysis
Shigenori MITSUSHIMA Tsutomu IOROIYoshiyuki KURODAKensaku NAGASAWATomoki UCHIYAMAYuki ORIKASAHiroshi INOUEEiji HIGUCHIKota ANDOTakashi NAKAJIMARyuta MISUMIYoshiharu UCHIMOTO
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2025 年 93 巻 4 号 p. 046001

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Toward decarbonized society with sustainable growth, the use of renewable energy as a primary power source is highly demanded. Water electrolysis is promising to produce hydrogen from renewable energy for energy storage and transportation. In developments of new technologies related to alkaline water electrolysis (AWE) and proton exchange membrane water electrolysis (PEMWE), common measurement techniques are required to compare experimental results fairly among different institutes. In this paper, we introduce common measurement techniques, such as electrochemical half cell and full cell for AWE and PEMWE, evaluation techniques for catalytic activities and durability of catalysts under steady and non-steady operation, advanced synchrotron radiation analysis of catalysts, operando XAFS analysis, and optical observation of gas bubbles in detail, that are recently developed in the project research commissioned by the New Energy and Industrial Technology Development Organization (NEDO).

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© The Author(s) 2025. Published by ECSJ.

This is an open access article distributed under the terms of the Creative Commons Attribution-NonCommercial-ShareAlike 4.0 License (CC BY-NC-SA, https://creativecommons.org/licenses/by-nc-sa/4.0/), which permits non-commercial reuse, distribution, and reproduction in any medium by share-alike, provided the original work is properly cited. For permission for commercial reuse, please email to the corresponding author. [DOI: 10.5796/electrochemistry.25-00046].
https://creativecommons.org/licenses/by-nc-sa/4.0/
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