Journal of the Ceramic Society of Japan, Supplement
Online ISSN : 1349-2756
ISSN-L : 1349-2756
Journal of the Ceramic Society of Japan, Supplement 112-1, PacRim5 Special Issue
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Yttria Partially Stabilized Zirconia Made by High-Speed Centrifugal Compaction Process
Hiroyuki Y. SUZUKIYuya NARAShunzo TASHIMAHidenori KUROKI
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Tetragonal zirconia polycrystal (TZP) compact was made via colloidal processing by the high-speed centrifugal compaction process (HCP). A pure zirconia powder of 0.14 μm was prepared into aqueous slip and compacted by the HCP under 10,000 g. The compact was presintered, then yttria phase stabilizer was impregnated in the form of an aqueous solution of yttrium nitrate.
The slip with the maximum powder concentration (72.2 mass%) yielded the highest green density of 46% and suppressed the segregation of particles during the HCP. The yttria-doped specimens were densified up to 99% at 1623 K without pressure assistance. The microstructure consisted of grains of 0.5 μm diameter of the tetragonal phase. The highest values of hardness and fracture toughness, Hv 1270 and 9.1 MPa m1/2, respectively, were obtained with a specimen doped with 2.7 mol% yttria.
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© 2004 The Ceramic Society of Japan
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