日本結晶成長学会誌
Online ISSN : 2187-8366
Print ISSN : 0385-6275
ISSN-L : 0385-6275
解説
A-μ-PD法による難加工性合金の線材結晶化技術
横田 有為吉川 彰
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2022 年 49 巻 2 号 論文ID: 49-2-05

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  We developed a novel fabrication method for alloy crystal fibers with poor-workability by unidirectional solidification using an alloy-micro-pulling-down (A-μ-PD) method and ceramic crucibles with sufficient mechanical and thermal shock resistance. Ir, Pt, Ru and their alloy fibers were fabricated from the melt directly by the A-μ-PD method. Long alloy fibers could be obtained using a pinch-roller and winding machine. Ir and Ru fibers were composed of number of elongated grains oriented along a growth direction which is attributable to the unidirectional solidification. In addition, microstructure and mechanical properties of Co-Cr-Mo (CCM) alloy fibers fabricated by the A-μ-PD method could be controlled by the growth rate. Ratio of the fcc-γ-phase in the CCM alloy fibers systematically increased with increasing growth rate. The hcp-ε-phase CCM crystal fibers exhibited considerably improved strain because of the slipping line in the hcp structure.

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