日本食品化学学会誌
Online ISSN : 2189-6445
Print ISSN : 1341-2094
ISSN-L : 1341-2094
論文
ポリカーボネート製器具・容器包装の溶出試験における ビスフェノールA 分析法の室間共同実験
片岡 洋平六鹿 元雄阿部 智之阿部 裕安藤 景子石原 絹代牛山 温子内山 陽介大坂 郁恵大野 浩之風間 貴充木村 亜莉沙佐藤 環高橋 良幸田中 葵棚橋 高志谷 拓哉照井 善光外岡 大幸永井 慎一郎野村 千枝花澤 耕太郎羽石 奈穂子早川 雅人平林 尚之藤吉 智治四柳 道代渡辺 一成佐藤 恭子
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ジャーナル フリー

2022 年 29 巻 3 号 p. 134-145

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An inter-laboratory study involving 23 laboratories was conducted to validate the government-approved analytical method for the determination of bisphenol A migrating from polycarbonate food processing materials. The obtained values were analyzed statistically using internationally accepted guidelines. Horwitz ratios were calculated based on the reproducibility relative standard deviation (RSDR), which was estimated from the inter-laboratory study, and predicted RSDR, which was calculated using the Horwitz/ Thompson equation. The analytical methods used for the migration solutions of water, 20% ethanol, and 4% acetic acid met the performance criteria of less than 2 of HorRat value set by the Codex Alimentarius for analytical method approval, but the analytical method for the migration solution of heptane did not. The results showed that the analytical method for the migration solution of heptane needs to be improved.
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