粉体および粉末冶金
Online ISSN : 1880-9014
Print ISSN : 0532-8799
X線回折によるMg-PSZ中の正方晶相の定量
土屋 信次郎土屋 一彦福田 雅秀宮谷 和雄
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42 巻 (1995) 9 号 p. 1059-1062

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A quantitative analysis of the tetragonal phase in Mg-PSZ by a standard X-ray powder diffraction method was carried out using the diffraction intensities with the Miller indices (311). The volume fraction of the tetragonal phase is shown to be given by
Vt=2.92/(1+0.991 X), where X={It(311)+Ic(311)}/It(113) which involves the diffraction intensities It and Ic of the corresponding tetragonal and cubic phases. The standard error of this method was estimated to be 4.5%. The present result is applicable to evaluate the tetragonal phase and the cubic phase in Mg-PSZ which contains the monoclinic phase less than 37%.

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