2004 Volume 45 Issue 7 Pages 2288-2294
The current study was conducted to develop a Ti-6Al-4V alloy composite material with a fine structure with improved mechanical properties by precipitating TiC particles via reaction-sintering and, additionally, by incorporating the effects of hydrides formed by hydrogenation treatment, using powder to which Mo2C had been added. The effects of precipitated TiC particles, and the subsequent generation of hydrides by hydrogenation treatment, heavy-strain working, and recrystallization treatment on grain refinement during the forming process were studied by means of structural observations. Warm rolling and multi-axial alternate forging (MAF) were employed as the heavy-strain working methods. The base metal structure of the Ti-6Al-4V composite material prepared by hydrogenation treatment on the sintered body prepared by spark plasma sintering (SPS) contains particles with a grain size not greater than 1 μm, which become finer with increasing hydrogen content. The particle size of TiC formed by reaction sintering, however, is not changed by heavy-strain working after hydrogenation. Its room temperature tensile strength increases with the amount of TiC precipitation, and is higher than that of non-hydrogenated material.