MATERIALS TRANSACTIONS
Online ISSN : 1347-5320
Print ISSN : 1345-9678
ISSN-L : 1345-9678
Determination Approach of Dislocation Density and Crystallite Size Using a Convolutional Multiple Whole Profile Software
Kodai MurasawaMasato TakamuraMasayoshi KumagaiYoshimasa IkedaHiroshi SuzukiYoshie OtakeTakayuki HamaShinsuke Suzuki
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2018 Volume 59 Issue 7 Pages 1135-1141

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Abstract

Neutron diffraction profile analysis using the whole profile fitting method is useful for obtaining microscopic information on metallic materials. To determine an appropriate fitting approach for obtaining reasonable and non-arbitrary results, we applied diffraction line profile analyses using the Convolutional Multiple Whole Profile (CMWP) method to diffraction patterns obtained using the Engineering Materials Diffractometer (TAKUMI, BL19) at the Materials and Life Science Facility (MLF) of the Japan Proton Accelerator Research Complex (J-PARC). The tensile specimens of 780 MPa grade bainitic steel were uniaxially stretched until the plastic strain reached a value of 0.05. We performed CMWP analyses on the obtained diffraction patterns during tensile test with various initial parameters of dislocation density and crystallite size. These parameters were optimized in the fitting procedures to minimize the weighted sums of squared residuals (WSSRs). Following this approach, we found that unsuitable initial parameter values resulted in unreasonable convergence. Therefore, initial fitting parameters should be chosen to ensure that the initial profiles are as broad as possible. Reasonable results were obtained following this suggestive approach even when the strain anisotropy parameter is set to arbitrary values.

Fig. 8 Converged dislocation density ρ and crystallite size L0 at various strain anisotropy parameter q. (a) Comparison among all the analyses results. (b) Comparison between before tensile tests without stress relaxation and with stress relaxation. (c) Effect of stress relaxation. In (b) and (c), pairs of (q, WSSR) are shown and underlined ones are of tensile tests with stress relaxation. Fullsize Image
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© 2018 The Japan Institute of Metals and Materials
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