Tetsu-to-Hagane
Online ISSN : 1883-2954
Print ISSN : 0021-1575
ISSN-L : 0021-1575
Regular Article
Determination of Nitrogen in Steel by Silent Discharge Molecular Emission Spectrometry after Fusion in Argon
Satoshi Kinoshiro
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2017 Volume 103 Issue 9 Pages 524-527

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Abstract

Helium is a noble gas that has some important properties, such as low boiling point, low density, high thermal conductivity, and inertness. Thanks to its unique properties, helium is widely used in various areas of science and technology. But its price has risen steadily every year since its supply shortage has arisen in 2012. In the steel industry, helium is used as a carrier gas for thermal conductivity method which can analyze nitrogen in steel accurately and quickly. Therefore it is necessary to develop a nitrogen analysis method in steel without using helium as preparation for its shortage. We have developed new analytical method which enables highly precise and rapid quantitative analysis of nitrogen contained in steel by using argon instead of helium. The developed method is based on discharge molecular emission spectrometry, and its quantitation limit of nitrogen in steel was 8 mass ppm.

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© 2017 The Iron and Steel Institute of Japan

This article is licensed under a Creative Commons [Attribution-NonCommercial-NoDerivatives 4.0 International] license.
https://creativecommons.org/licenses/by-nc-nd/4.0/
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