YAKUGAKU ZASSHI
Online ISSN : 1347-5231
Print ISSN : 0031-6903
ISSN-L : 0031-6903
イミダツォイソヒノリン誘導体の合成研究 (第1報)
9, 10-Dimethoxy-3-(p-aminophenyl)-5, 6-dihydrobenzoglyoxalocolineの合成
龜谷 哲治飯田 英夫
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1950 年 70 巻 5 号 p. 258-261

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4-Nitrohippuro-β-veratrylethylamide was obtained by the condensation of homoveratrylamine and 4-nitrohippuric acid azide. The dehydration of the amide in toluene with POCl3 gave, instead of 1-nitrobenzamidomethyl-6, 7-dimethoxy-3, 4-dihydroisoquinoline, a compound with a further loss of one mol. of water from it. The nitro derivative was reduced catalytically.

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