1954 年 74 巻 9 号 p. 961-962
Microdetermination of sulfanilamides was established by measuring by azotometric method the nitrogen gas generated from the reaction of the diazonium salt of sulfanilamide with sodium azide in an acid medium. The results of determination of several sulfanilamides agreed well with the results of diazo titration. Optimal determination range: 4×10-6-5×10-7M.