シクロヘキシルスルファミン酸塩に関する研究 (第3報)
ニトリドトリスルホン酸金属塩とシクロヘキシルアミンとの反応 その1
1961 年 81 巻 11 号 p. 1540-1543
詳細
1961 年 81 巻 11 号 p. 1540-1543
Metal nitridotrisulfate and cyclohexylamine are comparatively difficult to react than ammonium nitridotrisulfate and cyclohexylamine. Reaction at 170° under high pressure afforded 3 moles of cyclohexanesulfamate from 1 mole of ammonium nitri-dotrisulfate, but only 1 mole of cyclohexanesulfate was obtained from 1 mole of metal nitridotrisulfate.
Three new kinds of analogous compounds, C6H11NH2HN(SO3HC6H11NH2)2, C6H11NH2-HN(SO3Na)2, and C6H11NH2HN(SO3)2Ca, were prepared and their properties were examined.
