YAKUGAKU ZASSHI
Online ISSN : 1347-5231
Print ISSN : 0031-6903
ISSN-L : 0031-6903
Diphenyl Etherの研究(第7報)3-Chlorodibenz[b, g]-[1,5]oxazocine誘導体の合成
田中 悟緒方 善武
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1973 年 93 巻 8 号 p. 1003-1007

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Condensation of 4-chloro-2, 2'-di(bromomethyl)diphenyl ether (X) and ω-aminoalcohol (XI) gave 3-chloro-6-(ω-hydroxyalkyl)-6, 7-dihydro-5H-dibenz[b, g][1, 5]oxazocine (XII), with a 16-membered ring dimer (XIII) as a by-product. The formation ratio of these two products varied with reaction conditions. 3-Chloro-6(ω-alkylaminoalkyl)-6, 7-dihydro-5H-dibenz[b, g][1, 5]oxazocine (XV) was also synthesized.

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