It is effective for the maintenance of existing structures to understand the current status, such as the residual stress of the materials used, and a portable X-ray diffractometer is used as a technique for measuring steel stress. Although measurement methods and pre-treatment for steel bars with low strength have been revealed, the influence of the strength on the X-ray stress measurement and the appropriate measurement method has not been clarified. In this study, residual stress measurements using the X-ray diffraction are performed on steel bars, the differences in the results for various steels with different strengths are discussed, and measurement conditions for accurate measurement are reported. In addition, the cause of the tendency of the X-ray stress measurement to be smaller than the actual increment value under high stress is investigated. The experimental results show that the appropriate measurement conditions vary depending on the rebar strength, and that the X-ray stress measurement under high stress also varies. The metallurgical structure of the steel was shown to be related to the cause of this phenomenon through microstructural observation and analysis of the deformation behavior.
Cementitious materials generally have large carbon footprints because of the high CO2 emitted during Portland cement production. This is because limestone is used as an essential CaO resource, and its decomposition by calcination emits CO2. From this perspective, the concrete in urban buildings can be considered an urban mine of CaO resources. In this study, we propose obtaining a solidified product by crushing all the waste concrete, carbonating it, pressurizing it with a calcium bicarbonate solution, and drying it. The experimental results show that the bicarbonate solution, high-temperature conditions, and extended loading period produce a higher strength. In addition, neck growth at the contact surfaces of the carbonated concrete fines was confirmed using scanning electron microscopy. Consequently, the proposed method indicates that the hardening mechanism is the cold sintering of calcium carbonate on the surface of fine-carbonated concrete particles. This method allows the developed blocks to be used semi-permanently with relatively low energy consumption through repeated crushing and re-pressurization.