This report deals with the methods of preparation and standard evaluation of some sample of gases, such as NO
2, SO
2, H
2S, Cl
2, NH
3 and CO
2 that can not be prepared by use of their vapor pressure. As the standard method, diazotizing method for NO
2, p-rosaniline formaldehyde method for SO
2, methyleneblue method for H
2S, o-tolidine method for Cl
2, Nessler method for NH
3 and barium hydroxide method for CO
2 were adopted. The results obtained from the present standard evaluation method were in good accordance with those obtained from the experiment using Kitagawa's detector tubes, and the evaluated values did not vary with the lot number of detector tubes.
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