For the purpose of observing microstructural change in cold rolled (at 20°C) titanium plate at higher temperature under the vacuum of 10
-5mm Hg, observation has been made using high temperature microscope.
The results obtained are as follows:
1) At the temperature of recrystallization and grain growth determined through the tensile test and microstructual observation on cold worked and annealed titanium plate, structural change has been observed under high temperature microscope which occured from the region of high deformation strain within grains.
2) Recrystallization temperature has been determined to be between 460° and 580°C, where structural change has been observed by high temperature microscope as well as changes in tensile properties in cold worked and annealed titanium plate after heating.
3) Makings observed within grains after cold work has been found to disappear at the high temperature of say 700°C where grain growth is observed.
4) Heavily etched α boundary has been found to be retained after α→β transformation point was exceeded, but new β phase region has begun to be observed.
5) Small amount of oxygen has been introduced into the polished but unetched specimen surface at 500°C upon heating. No microstructural change, however, has been observed.
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