Grain refining effects of TiB
2 dispersed alloys on aluminum were investigated. The TiB
2 dispersed alloys were synthesized by the reaction between titanium and AlB
2, and were added to molten aluminum at 1273 K as the grain refining agents. Excess amount of titanium or aluminum was added to starting materials of the reaction for the purpose of controlling the adiabatic temperatures. In this paper, (1) distribution of TiB
2 particles in molten aluminum, (2) effects of TiB
2 distribution on the grain size and (3) mechanical properties of grain-refined aluminum are mainly dealt with. Since aluminum oxide forms at the inter-particle regions of TiB
2, the dispersion of TiB
2 particles in molten aluminum is not homogeneous when aluminum was added in the starting materials. The excess titanium addition as a diluent, however, improves the distribution of TiB
2 particles. The average grain size of aluminum alloy is effectively reduced by adding the TiB
2 dispersed alloy. The grain refining effects are saturated by about 0.4 vol% addition of TiB
2 particles. The 0.2% proof stress of Al–2 mass%Mg alloy is improved by the grain refining.
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