日本応用磁気学会誌
Online ISSN : 1880-4004
Print ISSN : 0285-0192
ISSN-L : 0285-0192
10 巻, 2 号
選択された号の論文の80件中51~80を表示しています
磁性体物理
薄膜
  • 鈴木 義茂, 増田 治訓, 芝田 次男, 腰塚 直己
    1986 年 10 巻 2 号 p. 279-282
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    A series of compositionally modulated Nd-Co thin films was prepared by UHV evaporation. The modulated structure and composition of the films were studied by X-ray diffraction measurement and energy dispersive X-ray microanalysis, respectively. Magnetization and anisotropy measurements were carried out using a vibrating sample magnetometer in the temperature range between 77 K and room temperature. A coherent structure was found over the modulation length, Λ, range 20 Å ≤ Λ ≤ 70 Å. The magnetization of the films with an atomic ratio of Nd : Co=1 : 3 changed slightly with Λ, but the perpendicular anisotropy energy decreased significantly with increasing Λ. The reduction of the anisotropy energy seems to be due to a decrease in the amount of atoms which are adjacent to the interfaces between Nd and Co layers.
  • 中山 則昭, 片元 勉, 新庄 輝也, 高田 利夫
    1986 年 10 巻 2 号 p. 283-286
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Multilayered films are prepared by the alternate deposition of Mn and Sb in ultrahigh vacuum. On deposition, Mn atoms react with Sb atoms to form a ferromagnetic compound MnSb at the interface. The MnSb layers grow epitaxially on thick Sb layers. By utilizing this epitaxy, ultrathin (less than 10Å) MnSb layers are sandwiched between thick (50Å) Sb layers. The resulting superlattice films are ferromagnetic even when each MnSb layer thickness is less than 5Å.
  • 小園 裕三, 小室 又洋, 成重 真治, 華園 雅信
    1986 年 10 巻 2 号 p. 287-290
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Multilayered structures and magnetic properties were studied for multilayered Fe/Cu films prepared by rf-magnetron sputtering method. Thickness of each Fe and Cu layer was 2.5, 5.0, and 10 nm, and the total thickness of Fe layers was 100 nm. When the thickness of Fe and Cu layers was less than 5 nm, Cu-Kα X-ray diffraction patterns showed one reflection at 2θ=44.1 degrees, which was intermediate between bcc Fe (110) and fcc Cu (111). Auger electron spectroscopy analysis and transmission electron microscopy (TEM) observation of a cross-section of these films showed periodic multilayered structure. The magnetic anistropy in the plane of multilayered Fe/Cu films was more remarkable than that of 100 nm Fe single layer film, and the coercivity decreased as thickness of the Fe and Cu layers decreased.
  • 片山 利一, 粟野 博之, 西原 美一
    1986 年 10 巻 2 号 p. 291-294
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Magnetic and magneto-optical properties of amorphous Zr-Fe/Tb-Fe composition modulated multilayered films (CMF) prepared by RF sputtering technique were investigated. In this system, a composition modulation period (D) more than 40 Å was confirmed by the low angle X-ray diffraction method. Curie temperature (Tc) of these multilayered films falls with decreasing D, but saturation magnetization (Ms) and perpendicular anisotropy (Ku⊥) increase with decreasing D. Sharpening of hyperfine field distribution was observed with the decrease of D. Wavelength dependences of magneto-optical Kerr rotation (θK) are independent of the variation of D.
  • 光岡 勝也, 熊谷 昭, 成重 真治, 華園 雅信, 榊原 正彦
    1986 年 10 巻 2 号 p. 295-298
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Magnetoresistive effect, effective anisotropy field, domain patterns and reading abilities were studied in improved type sensors made of high magnetoresistive Ni-Co films with auxiliary pole of Ni-Fe films. Demagnetizing field in improved type sensors with the same Ni-Co stripe width as conventional type sensors was reduced to half that of the latter. Under an angular change of applied field or an application of low bias field, magnetoresistive effect in conventional type sensors decreased. This was caused by the existence of domain walls. On the other hand, improved type sensors were composed of a single domain; therefore, magnetoresistive effect did not decrease under the same field conditions. Read-out value for magnetoresistive effect of improved type sensors is about 1.6-1.8 times greater than that of conventional type sensors. The ratio of the stripe width of the sensors to the recording bit length was found to be an important factor in enlarging the distance from a medium to the sensors.
  • 永田 裕二, 深沢 利雄, 青井 孝久
    1986 年 10 巻 2 号 p. 299-302
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Magnetoresistive (MR) effect and anisotropy field (Hk) of NiFe thin film annealed in a direct and rotational magnetic field were studied. In the large size MR element, Hk decreased with temperature up to 300°C due to stress relaxation. When the annealing temperature exceeds 350°C, both Δρ/ρ vs. H curves measured along magnetic hard and easy axis showed large dispersive hysteresis. This resulted in a decrease in Δρ/ρ. In the fine stripe MR element, on the contrary, magnetoresistive and magnetic properties of NiFe film hardly changed at temperature up to 500°C because of shape magnetic anisotropy.
    An MR head with magnetic yoke constituted of amorphous CoNbZr was fabricated. The MR head was annealed in a direct and rotational magnetic field in order to obtain high permeability of the yoke. MR characteristics of NiFe film located in the head had a desirable response.
  • 玉浦 裕, 後藤 吉孝, 五味 学, 阿部 正紀
    1986 年 10 巻 2 号 p. 303-306
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Polycrystalline Fe3O4- and Co-ferrite films were plated on glass- and PET-substrates by a modified method of the electroless ferrite-plating technique, “thin liquid-film (TLF) method.” Aqueous solutions (reaction solution, oxidizing solution) were flowed through the reaction cell (22 × 7 mm2, space ∼ 10 μm) in which the substrate had been placed. The reaction was influenced by the flow rates of the reaction solution (vr) and oxidizing solution (vo), flow time (tf) of the oxidizing solution, interval of the flow (ti) of the oxidizing solution, reaction temperature (T), concentration of the dissolved oxygen in the oxidizing solution (partial pressure of the oxygen in the air/N2 gas passed through the oxidizing solution, pO2), and reaction pH. Under the condition where vr, vo=15ml/min, tf=1 s, and ti=20 s, effects of T, pO2, and pH on the ferrite plating reaction were studied.
  • 高橋 研, 諏訪部 繁和, 成田 隆之, 脇山 徳雄
    1986 年 10 巻 2 号 p. 307-310
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Fe-Si (0∼16 wt% Si) and Fe-Si-Al (3∼14 wt% Si, 0∼8 wt% Al, bal Fe) alloy films have been prepared by DC sputtering technique. In Fe-Si films, the equilibrium phase expected from the phase diagram could be obtained under the sputtering condition (PAr=40 mTorr, VDC=3.5 kV), while under a different sputtering condition (PAr=40 mTorr, VDC=2.0 kV ), disordered α-phase as a non-equilibrium phase could be realized up to about 16 wt% Si. Concentration dependence of the magnetostriction, λ, for Fe-Si films sputtered under VDC=3.5 kV was found to be nearly the same as that of bulk crystals. However, for Fe-Si films consisting of the α-phase, the sign of λ remains positive up to about 16 wt% Si. Concentration dependence of zero magnetostriction, λ=0, determined for Fe-Si-Al films is found to be different from that of bulk crystals and also different from that of the evaporated films reported by Kadono et al.. Comparing the concentration dependence of λ with that of magnetocrystalline anisotropy constant, K1, determined by the present authors, it is proposed that the films with soft magnetic properties such as Sendust alloy be realized in the Fe-rich concentration portion.
  • 今野 正樹
    1986 年 10 巻 2 号 p. 311-314
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    The magneto-optical properties and related magnetic properties were studied for a series of polycrystalline Fe-Ni Invar films prepared by a vacuum evaporation method. The Kerr rotation angle (θK) was measured through a glass substrate by the polar Kerr magneto-optic effect using a He-Ne laser (6328 Å). The Kerr rotation angle of Fe71Ni29 increases from 0.032° to 0.165° with decreasing film thickness from 360 Å to 200 Å. However, there is little decrease of θK at the top surface boundary of the film. Therefore, the increase of θK is believed to be caused by the increase of magnetic moment at the bottom boundary. It is concluded that the interaction between film and substrate is a very important factor in the thickness dependence of the magnetic moment of Invar alloy film (∂MS/∂D < 0).
  • 星 陽一, 直江 正彦
    1986 年 10 巻 2 号 p. 315-318
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Iron-cobalt alloy thin films (0-54 at.% Co-Fe) were deposited using an ion beam sputtering apparatus and their magnetic properties were investigated in detail.
    All of the films have large saturation magnetic flux density above 20 kG. The films deposited at substrate temperature Ts of about 75°C have a large perpendicular magnettc anisotropy field Hk⊥ (>110 Oe) and high coercive force Hc (>50 Oe), while the increase of Ts shows a significant decrease in both Hk⊥ and Hc. The perpendicular magnetic anisotropy of the film deposited at Ts above 250°C disappears completely, and films with Co content of 50-54at.% have the lowest Hc, as low as 5 Oe. The decrease of Ts from 75°C to 250°C also causes a change in the internal stress of the films from compressive to tensile stress along with a growth of crystallites. Annealing the films in a vacuum has nearly the same effect on changes of their magnetic properties and internal stress as the increase of Ts. These changes in magnetic properties with Ts or annealing temperature are considered mainly caused by the change of stress induced magnetic anisotropy energy, since the Fe-Co alloy film has a large positive magnetostriction constant.
  • 太田 聡, 寺田 章
    1986 年 10 巻 2 号 p. 319-322
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    RF reactive sputtering discharge condition was studied by the measurement of temperatures. A thermocouple was set between a target and a substrate. Temperature rapidly changed at critical RF power (Pf1, and Pf2) in an Ar-O2 mixed atmosphere, though such a charge was not observed in an Ar atmosphere. Deposition rate, structure and magnetic properties for the sputter-deposited films also abruptly changed at the critical point of Pf1 and Pf2. The Pf1 and Pf2 increased with an increase of oxygen partial pressure. The critical RF power, however, decreased with an increase of total pressure, increasing the temperature values. These experimental results were qualitatively explained by an oxidation of the target surface
  • 清水 正二, 秦泉寺 哲, 加島 篤, 見山 友裕, 藤井 壽崇
    1986 年 10 巻 2 号 p. 323-326
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    In an attempt to fabricate transparent ferromagnetic materials coexisting with ferroelectricity above room temperature, we have examined reactive rf-sputtered films of solid solution compounds with (BiFeO3)1-x(PbTiO3)x, x=0 to 1. The targets were mixed powders of Bi2O3, α-Fe2O3, PbTiO3 and PbO, in which the first two components were used to synthesize BiFeO3 by 1 : 1 mixing in mol. % and the last component was added by 5 mol. % with respect to PbTiO3 to compensate the evaporation loss of lead during sputtering. As-grown samples deposited at about 400°C are amorphous but have noticeably large saturation magnetization 4πMs=210 G and saturation dielectric polarization of Ps=0. 092 μC/cm2 at room temperature. The samples are turned into polycrystalline by post-heat treatment at 700°C for 2 hours in air and 4πMs is increased to about twice as large as the initial one, while Ps is, in most samples, rather decreased. The samples have a high transmittance in the wavelength of visible through near-infrared. The refractive index n of BiFeO3 film is 3.0 at λ=700 nm.
  • 小山 博之, 辻本 浩章, 白江 公輔
    1986 年 10 巻 2 号 p. 327-330
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    CoNbZr amorphous films have attracted the attention of many researchers because of their high saturation magnetization, high permeability, low coercivity, and nearly zero magnetostriction. For the application of these films, one of the important magnetic properties is the behavior of the permeability over a wide frequency range. We have measured the permeability of a square shaped magnetic film (13 mm × 55 mm) sputtered on a glass substrate from 1 MHz to 400 MHz using a stripline. Over 400 MHz, measurement of the permeability of the magnetic film has been made using a ring shaped sample mounted in a coaxial fixture. The wall motion permeability of CoNbZr amorphous films decreases from 1 KHz and becomes nearly zero at 1 MHz. The rotation permeability is constant to 100 MHz and the ferromagnetic resonance is observed near 1 GHz
磁気応用
生体磁気
  • 上野 照剛, 北原 隆宏, 原田 耕介, 塩川 光一郎
    1986 年 10 巻 2 号 p. 383-386
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    Possible influence of ELF (extremely low frequency) magnetic fields or electric fields on the early embryonic development of frogs was studied. African clawed toads, Xenopus laevis, were used. Embryos were exposed to 10-15 mT alternating magnetic fields at different frequencies (20 Hz, 2.0 kHz, and 20 kHz) either during cleavage to neurula stage or the neurula to tail bud stage. During field exposures, the embryos were bred in a cylindrical chamber filled with 1/5 diluted saline solution so that the eddy currents could be induced in the solution. The estimated current densities induced by the ELF magnetic fields were 0.01-10.5 μA/mm2. The results show that the magnetic fields exert no harmful or modifying effects on the embryonic development.
    In order to obtain the critical current density which gives rise to teratogenic effects, electrical currents were directly applied to the embryos. When the cleavage-stage embryos were exposed to 20Hz electric fields for 8 hrs, the current density of 100 μA/mm2 gave lethal value or 100% malformation. When the embryos were exposed to an alternating current of 100 μA/mm2 at 20Hz for 15 min in each stage, the cleavage-brastra-stage embryos were those mostly damaged by the field (91 % malformation).
  • 上野 照剛, 江崎 浩, 原田 耕介
    1986 年 10 巻 2 号 p. 387-390
    発行日: 1986/03/31
    公開日: 2007/12/27
    ジャーナル オープンアクセス
    The effects of magnetic fields on combustion velocity and combustion temperature of alchol with platinum catalysis were studied. The place of combustion reaction was exposed to d. c. magnetic fields with field intensities from 0.1 T to 1.0 T.
    Combustion velocity was defined as the mean velocity over the period from ignition to consumption of the fuel. The combution velocity was influenced by a specific magnetic field. The combustion velocity of methanol was observed to be decreased by -5.3% with the application of a magnetic field of 0.9 T.
    Instantaneous combustion temperature was measured continuously, before, during, and after magnetic field exposures. The temperature was measured by an infrared thermometer the sensor probe of which was kept a distance from the combustion place and connected to a PbS transducer through an optical fiber. The results show that the combustion temperature of methanol decreased gradually in accordance with the field exposures at 0.9 T.
    Fluctuation in temperature variation increased during field exposure of the same intensity (0.9 T).
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