The purpose of this study was to investigate the influence of etching times for the effect of acid etching on the primary enamel smooth surfaces.
Eighty-two labial surfaces of the extracted or exfoliated caries-free primary anterior teeth were used. The cleaning and polishing pretreatments used in this study were: application of 10% NaOCl (Neo Dental Chemical Products Co. ), polishing with a brush cone (Hawe-Neos-Dental Co. ), polishing with a brush cone and tooth paste (Lion Co. ), Neo-Polishing-Paste (Neo Dental Chemical Products Co. ) and pumice slurry (Tokyo Dental College prescription).
Etchant used in this study was 40% phosphoric acid gel and the etching times were 10,30 and 60 seconds. All specimens were washed with an air water spray for 30 seconds after etching.
The following observations were obtained using the SEM.
1. The shorter the etching time, the higher was the rate of the cases which did not show any prism structure.
2. The numbers of the cases which did not show any prism structure were: 2(8.3%) out of the 24 in 60 seconds etching,5 (16.7%) out of the 30 in 30 seconds etching and 8 (38.6%) out of the 28 in 10 seconds etching.
3. Especially in the cases pretreated with the 10% NaOCl solution and Neo Polishing Paste, the rate of the cases which did not show any prism structure increased with the shorter etching time.
4. The shorter the etching time, the lower was the rate of the cases which showed peripheral etching patterns, core etching patterns and peripheral and core etching patterns.
5. However, the rate of the cases which showed poorly structured etching patterns was high in all etching time.
6. In the etching times used in this study,60 seconds is an adequate time for etching on the unground primary enamel smooth surfaces.
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