Separation of carrier free206Bi from the206Pb target bombarded by 19 MeV deuteronparticles obtained from the 160-cm IPCR cyclotron was studied. The bombarded lead nitrate (enriched206Pb (NO3) 2) was dissolved in 0.1 M nitric acid and 0.2 M oxine-TBP was added, and the two phases were mixed well by one minute shaking. The carrier free206Bi was separated by extraction with 0.2M oxine-TBP and then back-extracted into conc. HNO3.The recovery efficiency was about 95%. A carrier free206Bi with sufficiently high radiochemical purity was obtained by this simple procedure.
The fundamental studies were made on the selection of activable tracers which were usable to examine the distribution of agricultural insecticide sprayed by helicopter. Considering the conditions that the samples are organic substances, sufficiently strong radioactivity should be produced in a short irradiation-time, and the half life of the activity is desired to be longer than two hours for the sake of convenience of activity measurement, manganese, gold and europium were selected as typical tracers. Other conditions required for the field experiments were checked on these elements. Minimum detectable limits of each tracer was estimated from both the activity produced by each tracer and the background due to interference components in the sample. As a result, europium tracer was found to be the best in sensitivity (minimum detectable limit was 1.5×10-10gEu/5cm2filter paper) and also in cost, if the sampling was carried out using filter paper and a thin scintillator was used to measure low energy photons. After all, it was concluded that europium would be the most suitable tracer for the determination of distribution of insecticide sprayed by helicopter.
The rate constants of transperitoneal movement of urea in the peritoneal cavity were determined using14C-urea on six adult patients. It is considered that one half of the time consumed by the inflow and outflow of the solution is indifferent to intermittent peritoneal dialysis, and this length of time is defined as ineffective time. Peritoneal urea clearance can be expressed as a function of the dialysate flow rate, the ineffective ective time and the rate constant determined by this experiment. Optimal flow rate for various values of ineffective time can be estimated. To increase the efficiency of peritoneal dialysis, it it essentially important to shorten the ineffective time and also it is desirable to increase the dialysate flow rate to an optimal point which is dependent on the ineffective time in individual cases. When an intermittent peritoneal dialysis was performed using a litre of a solution per cycle, 28.4 minutes were required on an average for the inflow and outflow of the solution in the series of peritoneal dialyses. In order to obtain the maximum efficacy when one litre solution is used for one cycle, it is desirable that one cycle, from the beginning of the inflow to the end of the outflow, is completed in about 40 minutes.