In order to examine the time characteristics of a multi-wire 4πβ-counter for the 4πβ-γ coincidence system, measurement was made on the time distributions of the pulses from the individual anodes. The time distribution obtained by each anode was explained mainly by the distribution of primary ionizing position. A similar time distribution was obtained in the case that the alternating wires cathodes, when the individual anodes had the same effective detection region. Spurious pulses were observed in 90% argon plus 10% methane mixture at the end voltage of the plateau region and not methane gas.
A proportional control system was employed on this hygrometer. The hygrometer was used in a box in which the temperature and the humidity were constantly regulated. The range of measured dew-point was from -26°C to 60°C in the atmospheric temperature of 0°C to 60°C, that was the relative humidity of 12% to 100%, and the accuracy of the measurement was ±1°C.
The paper chromatographic behavior of tetranitronitrosylruthenate was examined together with its decomposition products. First, Rf values at various eluting conditions were studied with five kinds of papers, since there was a discrepancy among the reported Rf values. Usually R f of 0.9 was obtained by the recommended procedure of Wain, et al. Second, stability of the tetranitronitrosylruthenate in water was followed by paper chromatography. No change was found until 200 days passed. Third, the tetranitronitrosylruthenate was warmed in acid, and its decomposition products were studied through the paper chromatography. The paper chromatographic behavior showed that the sample kept in water more than 200 days seemed to contain a dinitro complex, and the sample warmed in acid seemed to be decomposed to a mononitro complex or further.
Nondestructive neutron activation analysis was performed on the nickel purified by floating zone-refining and anion exchange. It is found that floating zone-refining in vacuum is effective to remove Na, Sc, Cr, Zn, As, Ag, Sb and Hg through vaporization in addition to elimination of Se, Sb, Ta, Sm and Tb through segregation. Anion exchange method is also effective to separate Fe, Co, Zn, Mo, Hg, Th and U usually contained in the commercial nickel sources. It is concluded that combination of these two purification methods is required to obtain high purity nickel, since floating zone-refining is known ineffective to eliminate Fe and Co, main impurities in commercial nickel sources.