表面技術
Online ISSN : 1884-3409
Print ISSN : 0915-1869
ISSN-L : 0915-1869
75 巻, 6 号
選択された号の論文の8件中1~8を表示しています
小特集/接合技術および粒子積層技術のための表面性状制御
総説
解説
研究論文
  • 矢野 正明, 古賀 弘毅, 津留 豊
    2024 年 75 巻 6 号 p. 280-285
    発行日: 2024/06/01
    公開日: 2024/06/04
    ジャーナル フリー

    Zinc deposits obtained from the concentrated alkaline zincate bath always showed dendritic crystal. Whereas the bath added to Sn(IV)ion and/or In(III)ion inhibited dendritic crystal formation, the deposit obtained from the bath added to Sn(IV)ion showed block-like crystal formation. The deposit obtained from the bath containing In(III)ion showed a hexagonal, disc-shaped structure and steps on the edge of crystals, which led to the preferred orientation with the {10•2}, {10•3}, and {0•04} plane.

  • Sirorat TOOCHAROEN, Masayuki SHIMOJO
    2024 年 75 巻 6 号 p. 286-291
    発行日: 2024/06/01
    公開日: 2024/06/04
    ジャーナル フリー

    The nuanced interplay among focused electron beam(FEB)irradiation, tensile strain, and the ensuing craze development in polyethylene(PE)is examined. We designed and implemented rectangular irradiation patterns. The number, shape, and size of irradiation points were systematically varied, yielding intriguing patterns with distinct dimensions. In this study, irradiation was performed at an accelerating voltage of 5 kV, an electron beam current of 2 × 10−10 A, an irradiation time of 80 ms/point, and precisely controlled nominal tensile strains. The results demonstrated that FEB irradiation drastically influences the polymer microstructure and confirmed the formation of a rectangular craze. By altering the irradiation patterns from dots to rectangles, we successfully controlled the shape of the craze to realize a rectangular shape. At a nominal tensile strain of 15%, a distinct craze was observed, supporting the hypothesis that polymer irregularities influence craze formation as an effect of FEB irradiation. Size control experiments illustrated a linear correlation between the nominal strain and craze size. A key breakthrough was achieved in multiple craze control using FEB irradiation patterns. This research thus advances the understanding of precision-controlled craze formation, offering new possibilities for engineering materials with specific properties.

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