Journal of the Japan Society of Colour Material
Online ISSN : 1883-2199
Print ISSN : 0010-180X
ISSN-L : 0010-180X
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Volume 82, Issue 6
Displaying 1-6 of 6 articles from this issue
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Original Research Paper
  • Preparation of Carrageenan-Polyethyleneimine Nanocapsules Using Electrocapillary Emulsification Technique
    Hideki SAKAI, Hiroshi FUKUSHIMA, Mayumi SATOH, Tamotsu KONDO, Kenichi ...
    2009 Volume 82 Issue 6 Pages 231-236
    Published: June 20, 2009
    Released on J-STAGE: September 20, 2009
    DOIhttps://doi.org/10.4011/shikizai.82.231
    JOURNAL FREE ACCESS
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    The present paper proposes a novel preparation method of carrageenan-polyethyleneimine complex capsules in the submicron size range using the interfacial gelling reaction at W/O type emulsion. A W/O emulsion was prepared by adding dropwise aqueous τ-carrageenan solution into cyclohexane containing sorbitan monooleate through a microsyringe. Carrageenan gel particles were then prepared by adding the emulsion into a cyclohexane solution containing Ca AOT (calcium bis (2-ethylhexyl) sulfosuccinate) to cause gelation of aqueous droplets. The gel particles thus prepared were coated with polyethyleneimine to improve their stability in water. Capsules with sizes ranging from 100 to 300 nm were obtained when an apparatus for electrocapillary emulsification was used in the preparation step of W/O emulsion. The use of calcium salt of dimyristoyl phosphatidyl glycerol, a constituent of biomembrane, as gelling agent gave capsules of sizes in the submicron range.
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