Bulletin of the Society of Salt Science, Japan
Online ISSN : 2187-0322
Print ISSN : 0369-5646
ISSN-L : 0369-5646
Volume 5, Issue 4
Displaying 1-2 of 2 articles from this issue
  • Deposition of Gold and Silver on the Evaporation of Sea Water,(Salt Manufacture).
    Hiroshi Suzuki, Sakue Furihata, Seiji Nakamura
    1951Volume 5Issue 4 Pages 144-161
    Published: 1951
    Released on J-STAGE: May 17, 2013
    JOURNAL FREE ACCESS
    1. Detection of gold b/ means of SnCl2 solution.
    About known quantities of gold in 10 c. c. added 1 drop, of conc.HCl (1. 19) and 3 drops of sat. SnCl2 solution, detected by special gold brown Cassius reaction being specified its colour of blanc test. By this method, 0.01mg Au is detected.
    2. Gold contents in sea water.
    1 l sea water is treated by 1g Fe SO4 thoroughly, alkalified by 6n·NH4OH being converted Feto Fe and filtered.The ppt.is disso'ved by means of 6n HCl,washed thoroughly to chloride free. The filer paper is ashed,treated by 5 c. c. a uaregia,diluted With 5 c. c. H2O, evaporated to dryness, dissolved in 10 c. c. H2O and filtered. About f filtrate, gold is tested by means of theabove method.
    3, Gold deposition on the evaporation of sea water.
    16 brines of sample were prepared being concentrated from sea water to bittern. By means of the above method, gold contents of each samples were measured containing no gold in the brine sp.gr. 1.096, that is, all gold in sea water deposits when sea water is concentrated to its volume about 1/4 of sea water.
    4. Separation of gold by means of cupellation.
    (a) With 5g substance ppt.ed on the evaporation of seawater to the degree of sp.gr. 1.096, large bottom. of gold and silver alloy separated.(Au 0.75mg,Ag 2mg)
    (b) About scales, separated on common salt manufacture from sea water, only two scales containing mainly carbonate, Au and Ag alloy separated, the other scales consisting of CaSO4, no bottom separated.
    (c) Precipitants in the 1 st and 2 nd evaporating pond at soler salt field, sea: the bottom.
    (d) The transporting sand of Japanese salt field, separated the bottom.
    5. Absorption of Au in sea water.
    By means of three active carbons, Au in sea water abzorbed during 20min,at room temperature. Absorbed Au in carbon extracted about its 40% Au but contained its all quantities when the carbon is ashed.
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  • [in Japanese]
    1951Volume 5Issue 4 Pages 162-185
    Published: 1951
    Released on J-STAGE: May 17, 2013
    JOURNAL FREE ACCESS
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