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  • Joey
    B
    . Tanney, Leonard J. Hutchison
    Mycoscience
    2012年 53 巻 1 号 31-35
    発行日: 2012年
    公開日: 2023/03/31
    ジャーナル オープンアクセス

    The ability of Climacodon septentrionalis to immobilize and kill a mycophagous nematode (Aphelenchoides sp.) in vitro is described for the first time. Two isolates produced droplets (20–45 μm in diameter) that formed at the apices of tall, stalked, and branching secretory cells (700–

    1
    ,500 μm tall). On 2% modified malt extract agar, nematodes became enveloped in the droplets, which restricted their ability to move and resulted in complete immobilization and death within several hours of contact. The rate of decomposition of the nematodes varied considerably, with most individuals persisting for weeks whereas others were degraded within several days and appeared to be colonized by dense hyphal growth. This study provides the first documentation of a non-agaricoid fungus producing secretory cells that are able to immobilize nematodes.

  • M. L. GHOSH
    Journal of Physics of the Earth
    1972年 20 巻 2 号 165-186
    発行日: 1972年
    公開日: 2009/04/30
    ジャーナル フリー
    The possibility of attenuation of microseismic waves due to the presence of an upward folding of the ocean bottom into the liquid is discussed in this paper. The upward folding of the ocean bottom has been idealized by means of an irregularity in the form of a rectangle intruding into the liquid and the evaluation of the displacement component at any point of the solid medium has been carried out in two stages. First, the change in the incident mode of the surface wave due to the presence of the rectangular irregularity has been determined, and second, the subsequent change of the resulting displacement components due to the termination of the liquid layer and the step change in elevation of the solid medium at the continental margin has been discovered. Finally, numerical calculation has been made to determine the attenuation of the microseismic waves of different periods due to the presence of the rectangular irregularity at the ocean bottom.
  • A.M. BRITTO, C. SAVVIDOU, M.J. GUNN, J.R. BOOKER
    土質工学会論文報告集
    1992年 32 巻 1 号 13-25
    発行日: 1992/03/15
    公開日: 2008/02/29
    ジャーナル フリー
    One method currently being considered for the disposal of high level radio-active waste is burial in the seabed. When a hot object is buried in soil, the temperature of the soil adjacent to the object is raised and there is transient heat flow away from the object. The rise in the temperature of the soil causes excess pore pressures to be generated and transient pore water diffusion also takes place. A finite element formulation of the coupled heat flow and consolidation problem is presented. The computer implementation of this formulation is found to compare favourably with analytical solutions based on the same physical principles.
  • 増大する資源
    E
    . F. Boswell
    紙パ技協誌
    1998年 52 巻 7 号 885-889
    発行日: 1998/07/01
    公開日: 2009/11/19
    ジャーナル フリー
    The world is in the midst of a huge fundamental shift in fibre supply, demand balances, and policy changes. Governments around the world are introducing policy changes which influence the supply demand balance as the politicians' thoughts are uttered. Government agencies and their bureaucrats are imposing changes on industry even before the legislation is passed by the government in question.
    This ad hoc change process will continue for a time to come until the countries in question show a tough-mindedness with regard to their land use policies. Policies affecting forest areas such as protection areas, Native land claims, the protection of biodiversity and a true goal of sustainable development ; which addresses the combined issues of cultural, environmental, social and economic matters.
    Eventually all of these difficult issues will reach essential closure. Then there will be great new opportunities for investment to meet the growing demand for forest products ; leading to a strengthening competitive position in the more traditional producing areas such as Canada.
  • Grover Loening
    日本航空学会誌
    1963年 11 巻 119 号 373-380
    発行日: 1963年
    公開日: 2009/05/25
    ジャーナル フリー
  • S. Datta, J. Sil, M. K. Banerjee
    ISIJ International
    1999年 39 巻 10 号 986-990
    発行日: 1999/10/15
    公開日: 2007/05/31
    ジャーナル フリー
    The effect of composition and controlled thermomechanical process parameters on the mechanical properties of HSLA steels is modelled using the Widrow-Hoff's concept of training a neural net with feed-forward topology by applying Rumelhart's back propagation type algorithm for supervised learning, using a Petri like net structure. The data used are from laboratory experiments as well as from the published literature. The results from the neural network are found to be consistent and in good agreement with the experimented results.
  • 佐藤 敬之輔
    デザイン学研究
    1970年 1970 巻 11 号 45-55
    発行日: 1970/03/30
    公開日: 2017/07/25
    ジャーナル フリー
    [
    1
    ] The purpose of this reserch is to make clear what type of design can give good effects to win the high readership score. At the begining I had to know what factors decide the readership score, and how to change the quality of the desing into numerical value. I have used the method of multi-dimentional analysis with the help of a computer, and got the estimation formula, with
    7
    kinds of factors, as follows ; A^^〜=
    B
    +C+D+K+aE+
    bF
    +cG. A^^〜=estimated values of the readership score.
    1
    )
    B
    , C, D, K : these four factors are given as category values (so we call them); each factor is classified into several categories.
    B
    =week day, classified into
    7
    categories. C=pages of a newspaper, which are characterized by the kinds of articles, news, and the other reading matters, classified into
    22
    categories. D=kinds of goods and trades of the advertizement, classified into 14 catedories. K=constants, given to each 13 surveys. 2)
    E
    , F, G : these factors are given as numerical values. G=area of advertizement, measured by the unit of column in the whole page length, being classified into 6 kinds of area (2.5, 3.5, 5,
    7
    , 10, 15) and 15 column means a whole page, about 2,000cm^2.
    E
    , F are the marks obtained in the design of advertizements.
    E
    =sum of the marks obtained in each design element on the advertizement. F=the marks obtained on the whole effect of the design. 3) a,
    b
    , c : coefficients Using the above formula with the category values and the coefficients, we can obtain the naked design effect from the actual value A of readership score: aE+
    bF
    =A-(
    B
    +C+D+K+cG). In this research, I used
    1
    ,829 data of readership score from 1960 to 1968, being obtained by 13 survevs, spring and autumn twice a year. The sample of size each survey was 3,541, 2,251, or 200 in the other 11 surveys. Multiple correlation coefficient between the estimated value A^^〜 and the actual value A is
    0
    .951. The table 2^* shows the contribution indexes of each factor by 3 kinds of expression-(
    1
    ) Range : the absolute difference between the maximum and the minimum category values, (2) Standard deviations of the category values, (3) Partial correlation coefficient : the relationship between the actual values A and each factors. *see the table 2 in the thesis in Japanese. [2] The important point was in the determination of the values of
    E
    , F.
    E
    is the sum of the marks obtained in each design element, classified into four kinds :
    E
    =
    E
    _
    1
    +
    E
    _2+
    E
    _3+
    E
    _
    4
    . design elements [table]
    E
    _
    1
    ,
    E
    _2,
    E
    _3,
    E
    _
    4
    , these values have the 5 grades, as
    0
    ,
    1
    , 2, 3,
    4
    and
    0
    is given to the design that has no attractive effect or no applicable element. And
    E
    obtain the marks of
    0
    to
    9
    grades as the sum of them. The values of F have also 5 grades,
    0
    to
    4
    . The principles to determine the values of
    E
    , F are as follows : a) The marks obtained of
    E
    , F must be the relative values among the each survey, and at the same time, they must have constancy within the same survey-the same elements of design must win the same marks obtained.
    b
    ) They must be determined as to win the highest multiple correlation coefficient, when they are put into the estimation formula. c) They must be reasonable. In order to justify them, we must carry many researches on the actual condition. The frequency of accurence of each grade of
    E
    , F values, as the table 5-
    4
    , and 5-5 in the thesis in Japanese.
  • B
    .C. CHATTOPADHYAY, P.J. PISE
    土質工学会論文報告集
    1986年 26 巻 4 号 16-22
    発行日: 1986/12/15
    公開日: 2008/02/29
    ジャーナル フリー
    Horizontal plate anchors are widely used in civil engineering constructions to resist vertical pulling loads. The available theoretical model suggested by Vesic to estimate the breakout resistance of plate anchors is in significant error, particularly for dense sandy soils. A theoretical model assuming a curved surface of failure through the surrounding soil, to evaluate the ultimate breakout resistance of horizontal plate anchors, has been proposed. It successfully brings out the concept of characteristics relative depth beyond which the breakout factor reaches a constant final value. It is capable of predicting breakout factors for wide range of values of angle of shearing resistance of sand.
  • S. DATTA, M. K. BANERJEE
    ISIJ International
    2005年 45 巻 1 号 121-126
    発行日: 2005年
    公開日: 2006/01/27
    ジャーナル フリー
    An unsupervised learning technique and an associative memory have been used for encoding weights by a special type of Petri network named Petri neural net for modelling the influence of alloying elements on the final property of the high strength low alloy steel. The combined effects of alloying elements for different strengthening mechanisms is predicted when weights and threshold values are chosen on the basis of metallurgical understanding. The technique is found to be effective to create an associative memory of input-output relations in unknown data sets so that the same can be subsequently be used as a predictive tool.
  • S. Datta, M. K. Banerjee
    ISIJ International
    2004年 44 巻 5 号 846-851
    発行日: 2004/05/15
    公開日: 2007/05/31
    ジャーナル フリー
    Primarily from the point of view of improvement of yield strength due to additions of niobium, titanium and boron in HSLA steels, the experimental steels are divided into five classes. The data are then supplied for learning a Self Organising Map (Kohonen network). It is found that the network with six neurons possesses better capacity of prediction with unknown data. Another effort of clustering the steels according to its major strength contributing mechanisms is also made. But the capacity of the network to cluster unknown data is found to be rather poor and has failed to follow from the metallurgical principles. To avoid this limitation, Learning Vector Quantisation method is adopted to impart a certain amount of supervision in the learning process and it is found that the training pattern of the network attains a good convergence thereby leading to a good predictive ability.
  • M. K. Banerjee, P. S. Banerjee, S. Datta
    ISIJ International
    2001年 41 巻 3 号 257-261
    発行日: 2001/03/15
    公開日: 2007/05/31
    ジャーナル フリー
    A boron treated copper bearing HSLA steel containing austenite formers like manganese and nickel, somewhat lower in amount than that in HSLA 100 variety of steel is chosen for the study. The role of thermomechanical processing on the microstructure and mechanical properties of the above steel has been investigated. Differential scanning calorimetric study is carried out for understanding the precipitation behaviour of copper in HSLA steel under the influence of boron. The microstructure of the experimental steel is found to consist of laths of martensites and bainite. MA constituents of ribbon like morphology are observed at the lath boundaries. Higher strength properties of the steel are attributed to the presence of finely distributed precipitates of copper and microalloy carbides.
  • George W. Lee
    燃料協会誌
    1973年 52 巻 3 号 171-177
    発行日: 1973/03/20
    公開日: 2010/06/28
    ジャーナル フリー
  • Yilmaz ISPIR, Orhan UYAR
    Journal of geomagnetism and geoelectricity
    1971年 23 巻 3-4 号 295-305
    発行日: 1972/02/25
    公開日: 2010/09/14
    ジャーナル フリー
    Simultaneous measurements of the total geomagnetic field intensity by the same type of the proton precession magnetometers at two stations in NW Turkey have been taken cooperatively by a research group since December 1970. Up to the end of July 1971 mainly three probable local magnetic changes were observed. It was seen that after a decrease in the local field at a magnetic station (Erdek) a few earthquakes occured at either nearly N or S of that station, and after an increase in the local field an earthquake took place nearly W of the same station. In this paper the data and some results of the first part of observations are given.
  • その所属腱索および乳頭筋について
    島田 博
    日本医科大学雑誌
    1981年 48 巻 6 号 779-789
    発行日: 1981/12/15
    公開日: 2010/10/14
    ジャーナル フリー
    Although there have been numerous articles concerning the anatomy of the atrioventricular valve in man, only a few publications have recorded the relationship between the chordae tendineae and the papillary muscles. The purpose of this paper is to study the relationship among the shape and size of the atrioventricular valve, the chordae tendineae and the papillary muscles. 50 subjects, as listed in Table
    1
    , were analyzed by the Taniya-Hashimoto Method.
    The results obtained were as follows:
    1
    ) The right atrioventricular valve was classified into two types: 33 cases (66%) of three irregularly shaped cusps, i.
    e
    . type I, and 17 cases (34%) of four or five cusps, i.
    e
    . type II.
    2) The average circumference of the right atrioventricular orifice (ostium atrioventriculare dextrum) was 11.96cm (
    9
    .63.15.06cm) in type I and 12.19cm (
    9
    .52.15.
    22
    cm) in type H. There existed no significant difference in the circumference of the atrioventricular orifice between type I and II.
    3) The average length of the cusp-fundus (the length of the fixed margin of the cusp) was as follows:
    type I: anterior cusp…………
    4
    .13cm (2.03-6.96cm)
    posterior cusp…………3.62cm (
    1
    .21-5.44cm)
    septalcusp……………
    4
    .21cm (3.11-6.08cm)
    type II: anterior cusp…………
    4
    .10cm (2.68-5.42cm)
    posterior cusp…………3.67cm (
    0
    .
    94
    -5.70cm)
    septal cusp……………
    4
    .43cm (2.96-6.53cm)
    4
    ) The average width of the cusp (the maximum distance between the apex and the fundus of the cusp) was as follows:
    type I: anterior cusp…………
    1
    .86cm (
    1
    .26-2.29cm)
    posterior cusp…………
    1
    .62cm (
    0
    .62-2.
    94
    cm)
    septal cusp……………
    1
    .76cm (
    1
    .15-2.72 cm)
    type II: anterior cusp…………
    1
    .92cm (
    1
    .40-2.34cm)
    posterior cusp…………
    1
    .72cm (
    0
    .
    94
    -2.42cm)
    septal cusp……………
    1
    .84cm (
    1
    .14-2.53cm)
    The length or width of the cusp in type I was similar to that in type II.
    5) The papillary muscles consisted of five groups, which were named the anterior, postlateral, postmedial, postseptal and septal muscles. The average number of the papillary muscles per right ventricle was 5.
    7
    (2.
    0
    .
    9
    .
    0
    ). The chordae tendineae from the anterior papillarymuscles were attached to the anterior and posterior cusps and those from the postlateral and postmedial muscles were attached to the posterior and septal cusps. The chordae tendineae from the postseptal muscles were linked only to the septal cusp and those from the septal muscles were connected to the septal and anterior cusps.
    6) The average number of the stems of the chordae tendineae from the papillary muscles were as follows:
    From the anterior papillary muscles………
    7
    .2 (2.
    0
    -14.
    0
    )
    the postlateral papillary muscles……3.5 (
    1
    .
    0
    -8.
    0
    )
    the postmedial papillary muscles……
    4
    .
    0
    (
    1
    .
    0
    -8.
    0
    ) the postseptal papillary muscles……
    4
    .5 (
    1
    .
    0
    -13.
    0
    ) the septal papillary muscles………5.
    7
    (2.
    0
    -12.
    0
    )
    The average n umber of the stems of the chordae tendineae per right ventricle was 24.
    4
    (16.
    0
    -35.
    0
    ).
    7
    ) The tip of the chordae tendineae are attached to the fixed margin of the valve cusp, i.
    e
    . type A, to the ventricular surface, i.
    e
    . type
    B
    and to the free margin, i.
    e
    . type C. The average number of them were 23.
    4
    (14.
    0
    -32.
    0
    ) in type A, 19.2 (
    4
    .
    0
    -37.
    0
    ) in type
    B
    and 68.
    1
    (31.
    0
    -105.
    0
    ) in type C. The average number of the apexes of the chordae tendineae per right ventricle was 110.
    7
    (53.
    0
    -166.
    0
    ).
    8) The average number of the chordae tendineae for the anterior cusp was 34.
    9
    (12.
    0
    -64.
    0
    ), for the posterior cusp 30.5 (5.
    0
    -65.
    0
    ) and for the septal cusp 45.3 (23.
    0
    -68.
    0
    ).
  • 香山 滉一郎, 森下 政夫, 張 国鋒
    粉体および粉末冶金
    2006年 53 巻 5 号 419-429
    発行日: 2006年
    公開日: 2006/12/19
    ジャーナル オープンアクセス
    The phase diagrams of the Ni-Mo-
    B
    and Ni-W-
    B
    ternary systems in the region of less than 50mol%
    B
    were constructed by thermodynamic calculation, based on the data obtained by thermodynamic measurement of the related materials. We found three ternary eutectic points and three or two ternary peritecto-eutectic points as follows:
    E1
    :L (1365K, 71.5mol%Ni-6.
    0
    mol%Mo-
    22
    .5mol%
    B
    )=(Ni)+
    Ni3B
    +
    NiMo2B2

    E2
    :L (1355K, 62.5mol%Ni-2.5mol%Mo-30.5mol%
    B
    )=
    Ni3B
    +
    Ni2B
    +
    NiMo2B2

    E3
    :L (1445K, 42.
    0
    mol%Ni-30.6mol%Mo-10.3mol%
    B
    )=(Ni)+NiMo+
    NiMo2B2

    P1
    :L (1812K, 34.
    9
    mol%Ni-42.3mol%Mo-
    22
    .8mol%
    B
    )+MoB=
    Mo2B
    +
    NiMo2B2

    P2:L (1633K, 42.3mol%Ni-40.
    4
    mol%Mo-17.3mol%
    B
    )+Mo=
    Mo2B
    +
    NiMo2B2

    P3:L (1812K, 53.5mol%Ni-33.
    7
    mol%Mo-12.8mol%
    B
    )+Mo=NiMo+
    NiMo2B2

    E1
    :L (1622K, 51.
    0
    mol%Ni-31.6mol%W-17.
    4
    mol%
    B
    )=(Ni)+W+
    NiW2B2

    E2
    :L (1260K, 71.
    0
    mol%Ni-
    7
    .
    0
    mol%W-
    22
    .
    0
    mol%
    B
    )=(Ni)+
    Ni3B
    +
    NiW2B2

    E3
    :L (1291K, 65.
    4
    mol%Ni-
    4
    .8mol%W-29.8mol%
    B
    )=
    Ni2B
    +
    Ni3B
    +
    NiW2B2

    P1
    :L (2115K, 23.8mol%Ni-43.
    1
    mol%W-33.
    1
    mol%
    B
    )+WB=
    W2B
    +
    NiW2B2

    P2:L (1657K, 48.
    9
    mol%Ni-33.
    1
    mol%W-18.
    0
    mol%
    B
    )+
    W2B
    =W+
    NiW2B2

    The calculated phase diagrams are expected to be useful for the development of new Ni-based heat-, corrosion- or wear-resistance alloys.
  • Yukichi Yamaguchi, Jian-zhi Runan(Gen), Teruaki Nagahara
    Journal of the Physical Society of Japan
    1975年 38 巻 4 号 911-916
    発行日: 1975/04/15
    公開日: 2007/06/01
    ジャーナル 認証あり
    The gamma-ray spectrum and the conversion-electron spectrum are measured in the decay of the 116mIn activity. Directional correlations are also measured for 818–1293 and 1097–1293 keV cascades. The M
    1
    -
    E
    2 mixing ratio δ, and the
    E
    0
    -
    E
    2 mixing ratio μk are obtained for 818.
    7
    keV
    22
    +→21+ transition to be δ=
    1.52
    0.22
    +
    0.26
    , and μk≤6.
    1
    ×10
    4
    respectively. The
    E
    2 branching ratio
    B
    (
    E
    2;
    22
    +
    0g
    +):
    B
    (
    E
    2;
    22
    +→21+):
    B
    (
    E
    2;
    22
    +→01+) is determined to be
    0
    .0158:
    1
    .
    0
    :5.86.
  • MARIE LAVAULT, ALAIN FOURNET, HELENE GUINAUDEAU, JEAN BRUNETON
    Chemical and Pharmaceutical Bulletin
    1986年 34 巻 3 号 1148-1152
    発行日: 1986/03/25
    公開日: 2008/03/31
    ジャーナル フリー
    Nine isoquinoline alkaloids belonging to the protoberberine, proaporphine and bisbenzyl-isoquinoline series were isolated from Caryomene olivascens (Menispermaceae). Four compounds are new : (-)-2-norlimacine (
    4
    ), (-)-caryolivine (6), (+)-
    1
    , 2-dehydro-2-norlimacusine (
    9
    ) and N-formylstepharine (3). The last one is the first N-formyl derivative to be reported in the proaporphine group. Its biogenetic origin is discussed. Structures were established on the basis of 360 MHz (FT) nuclear magnetic resonance measurements and also by chemical correlation in the case of 3.
  • 松下 秀鶴, 嵐谷 奎一, 小谷野 道子
    大気汚染研究
    1976年 11 巻 4 号 252-259
    発行日: 1977/01/20
    公開日: 2011/08/11
    ジャーナル フリー
    This paper discribes a sample method for determining polynuclear aromatic hydrocarbons (PAH) in soil, This method consists of the following procedures. Soil samples are passed thruogh a screen of 28 mesh for removing fine stands and rubbish. PAH in the soil samples are extracted with 150 ml of benzene for 8 hours by with Soxhlet's appratus. The extracted benzene solution is then evaporated to dryness at low temperture (ca. 40°C) by a rotary evaporator. The residue is dissolved in a small volume of benzene. PAH in the benzene solution are separated into each component with one-dimensional dual band thinlayer chromatography [Thin-layer plate; Kieselguhr G (2×20, cm)-(26% Acetylated cellulose + Cellulose D-
    0
    ) (95: 5, w/w, 16×20, cm), Developer; Ethanol-Ether-Water (
    4
    :
    4
    :
    1
    , v/v) for the
    1
    st development, Methanol-Ether-Water (
    4
    :
    4
    :
    1
    , v/v) for the 2nd development]. Each PAH spot separated on the thinlayer is scraped off into a small centrifugal-tube. After adding
    4
    ml of dimethyl sulfoxide (DMSO) into a tube, ultra sonic extraction is carried out for 10 minutes in order to completely dissolve PAH into DMSO. This DMSO solution is centrifuged for 5 minutes. PAH in the supernatant is identified by comparison of its fluorescence and excitation spectra with those of standard PAH solution and determined spectrofluorometrically by narrow base line method. The accuracy of this method was high and stable. For example, recovery and its coefficient of variation was
    97
    .2% and
    1
    .01% for pyrene, 96.
    7
    % and
    1
    .58% for benz (a) anthracene, 95.
    7
    % and 2.06% for benzo (a) pyrene, and
    94
    .3% and
    1
    .58% for benzo (ghi) perylene.
    Authors applied this method to the analysis of PAH in soil, and 11 PAH were identified. They were pyrene, fluoranthene, chrysene, anthanthrene, benzo (
    b
    ) fluoranthene, benz (a) anthracene, benzo (a) pyrene, perylene, benzo (
    e
    ) pyrene and benzo (ghi) perylene. The identified PAH except benzo (
    b
    ) fluoranthene were also determined quantitatively. Benzo (a) pyrene contents in soils in urban areas were much higher than those in soils in rural areas. The contents were 53-4930 ppb in urban area and
    0
    .07-11 ppb in rural area. Benzo (a) pyrene contents in urban soils were higer in winter as compared with those in summer. PAH contents in soils which were sampled in Yotsuyakamimachi, Kawasaki-shi a heavy air pollution area in winter of 1973 were ranged from 3.33 to 65.
    0
    ppm for pyrene, from 3.09 to 70.
    7
    ppm for fluoranthene, from
    1
    .02 to 24.8 ppm for chrysene, from
    0
    .44 to 10.8 ppm for benz (a) anthracene, from
    0
    .
    94
    to
    22
    .
    1
    ppm for benzo (a) pyrene, from
    0
    , 29 to 8.
    94
    ppm for benzo (k) fluoranthene, from
    0
    .20 to
    4
    .95 ppm for perylene, from
    0
    .30 to 10.
    4
    ppm for benzo (
    e
    ) pyrene, from
    0
    .12 to 2.78ppm for anthanthrene, and from
    0
    .
    94
    to 14.
    9
    ppm for benzo (ghi) perylene. These findings suggest strongly the fact that soils in urban area are polluted by PAH including carcinogenic benzo (a) pyrene.
  • 黒川 美貴雄, 吉田 耕治, 永井 保嵩, 宇野 準
    Chemical and Pharmaceutical Bulletin
    1983年 31 巻 12 号 4312-4318
    発行日: 1983/12/25
    公開日: 2008/03/31
    ジャーナル フリー
    Two new partially saturated tricyclic ring systems, 6, 6a,
    7
    , 8,
    9
    , 10, 10a, 11-octahydro-11-oxodibenz [
    b
    ,
    e
    ] oxepins (3a and 3
    b
    ), and -thiepins (
    4
    a and
    4
    b
    ) were synthesized. Compounds
    4
    a and
    4
    b
    were desulfurized to give a pair of isomeric 2-methylbenzoylcyclohexanes (10a and 10
    b
    ). Deuterated
    4
    a and
    4
    b
    (11a and 11
    b
    ) were prepared starting from butadiene-d6 (12). The stereochemical features of 3a (trans), 3
    b
    (cis),
    4
    a (trans) and
    4
    b
    (cis) are compared with those of 10a, 10
    b
    , 11a and 11
    b
    on the basis of proton nuclear magnetic resonance data.
  • 世一 義隆, 上野 政一, 掛見 和郎
    分析化学
    1970年 19 巻 4 号 568-570
    発行日: 1970/04/05
    公開日: 2009/05/29
    ジャーナル フリー
    Cytosine arabinoside is in some circumstances
    e
    .g. by heating, converted into uracil arabinoside. A paper chromatographic method was recommended for the determination of cytosine arabinoside in the presence of uracil arabinoside in which a mixture of ethyl acetate, iso-propanol and water (2:2:
    1
    ) was used as the developing solvent on Toyo No. 5
    B
    or Whatman No.
    1
    filter paper (3 cm×20 cm). The method was rapid and accurate, and the calibration formula for cytosine arabinoside was 18.28A282-
    0
    .06 and that for uracil arabinoside was 23.70A264+
    0
    .09.
    The recovery of cytosine arabinoside in 2% aqueous solution after 6 hours heating in boiling water was:
    pH cytosine arabinoside %
    5.
    4
    94
    .6
    7
    .6
    97
    .
    9

    9
    .2
    97
    .
    4
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