Journal of The Adhesion Society of Japan
Online ISSN : 2187-4816
Print ISSN : 0916-4812
ISSN-L : 0916-4812
Original Paper
A Method to Chase Changes of Depth Profiles of Conversion in Thick Layers of UV Curable Resin Using Real-Time FT-IR Method
Yoichi NAMIKIChiaki AZUMAMasahiro YONENOTamotsu YAMAMOTO
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JOURNAL FREE ACCESS

2002 Volume 38 Issue 9 Pages 329-333

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Abstract
A method evaluating the time-course of depth profiles of conversion in thick layers of UV curable resins has been established. This method is based on chasing the curing reaction of the resin as the change of infrared absorbance at the absorption band assigned on its vinyl group, which is put on a horizontal ATR prism equipped in FT-IR spectrophotometer, under UV light irradiation vertical to the prism. From the real-time data at any depths, the time-course of depth profiles of conversion can be pictured. Using a methacrylic acid ester UV curable resin, the present evaluating method was exemplified.
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© 2002 The Adhesion Society of Japan
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